000 | 01706cam a22002415a 4500 | ||
---|---|---|---|
999 |
_c27250 _d27221 |
||
005 | 20190321094815.0 | ||
008 | 160917t2017 enka frb 001 0 eng d | ||
020 | _a9780128095812 | ||
040 |
_aIDEBK _beng _cIDEBK _dOCLCO _dUk _dEG-ScBUE |
||
082 | 0 | 4 |
_a547 _bPIR _222 |
100 | 1 | _aPirrung, Michael. | |
245 | 1 | 0 |
_aHandbook of synthetic organic chemistry / _cMichael C. Pirrung. |
246 | 3 | 0 | _aSynthetic organic chemistry |
250 | _a2nd ed. | ||
260 |
_aLondon : _bAcademic Press, / Elsevier, _cc.2017. |
||
300 |
_axii, 272 p. : _bill. (some col.) ; _c24 cm. |
||
504 | _aIncludes bibliographical references and index. | ||
505 | 0 | _a1. Safety<br>2. Searching the literature<br>3. Reagents<br>4. Gases<br>5. Reactions on a small scale -- 1-25 mmol<br>6. Temperature control<br>7. Solvents<br>8. The research notebook<br>9. Conducting the reaction itself<br>10. Following the reaction<br>11. Working up reactions<br>12. Evaporation<br>13. Vacuum systems<br>14. Purification of products<br>15. Methods for structure elucidation<br>16. Cleaning up after the reaction<br>17. Specific examples<br>18. Strategies for reaction optimization<br>Appendices<br>1. Safety protocols<br>2. Synthetic solvent selection chart<br>3. Solvent miscibility<br>4. Freezing points of common organic solvents<br>5. Toxicities of common organic solvents<br>6. Recipes for TLC stains<br>7. NMR spectral data of common contaminants of organic and organometallic reaction products<br>8. Acidities of organic functional groups<br>9. Acidities of organic functional groups in DMSO<br>10. Stuck joints | |
650 | 7 |
_aOrganic compounds _xSynthesis. _2BUEsh _941977 |
|
651 | _2BUEsh | ||
653 |
_bENGCHE _cMarch2019 |
||
942 | _2ddc |