TY  - BOOK
AU  - Pirrung,Michael
TI  - Handbook of synthetic organic chemistry
SN  - 9780128095812
U1  - 547 22
PY  - 2017///
CY  - London
PB  - Academic Press, / Elsevier
KW  - Organic compounds
KW  - Synthesis
KW  - BUEsh
KW  - ENGCHE
KW  - March2019
N1  - Includes bibliographical references and index; 1. Safety<br>2. Searching the literature<br>3. Reagents<br>4. Gases<br>5. Reactions on a small scale -- 1-25 mmol<br>6. Temperature control<br>7. Solvents<br>8. The research notebook<br>9. Conducting the reaction itself<br>10. Following the reaction<br>11. Working up reactions<br>12. Evaporation<br>13. Vacuum systems<br>14. Purification of products<br>15. Methods for structure elucidation<br>16. Cleaning up after the reaction<br>17. Specific examples<br>18. Strategies for reaction optimization<br>Appendices<br>1. Safety protocols<br>2. Synthetic solvent selection chart<br>3. Solvent miscibility<br>4. Freezing points of common organic solvents<br>5. Toxicities of common organic solvents<br>6. Recipes for TLC stains<br>7. NMR spectral data of common contaminants of organic and organometallic reaction products<br>8. Acidities of organic functional groups<br>9. Acidities of organic functional groups in DMSO<br>10. Stuck joints
ER  -