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Handbook of synthetic organic chemistry / Michael C. Pirrung.

By: Material type: TextTextPublication details: London : Academic Press, / Elsevier, c.2017.Edition: 2nd edDescription: xii, 272 p. : ill. (some col.) ; 24 cmISBN:
  • 9780128095812
Other title:
  • Synthetic organic chemistry
Subject(s): DDC classification:
  • 547 PIR 22
Contents:
1. Safety<br>2. Searching the literature<br>3. Reagents<br>4. Gases<br>5. Reactions on a small scale -- 1-25 mmol<br>6. Temperature control<br>7. Solvents<br>8. The research notebook<br>9. Conducting the reaction itself<br>10. Following the reaction<br>11. Working up reactions<br>12. Evaporation<br>13. Vacuum systems<br>14. Purification of products<br>15. Methods for structure elucidation<br>16. Cleaning up after the reaction<br>17. Specific examples<br>18. Strategies for reaction optimization<br>Appendices<br>1. Safety protocols<br>2. Synthetic solvent selection chart<br>3. Solvent miscibility<br>4. Freezing points of common organic solvents<br>5. Toxicities of common organic solvents<br>6. Recipes for TLC stains<br>7. NMR spectral data of common contaminants of organic and organometallic reaction products<br>8. Acidities of organic functional groups<br>9. Acidities of organic functional groups in DMSO<br>10. Stuck joints
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Holdings
Item type Current library Collection Call number Vol info Status Date due Barcode Item holds
Book - Borrowing Book - Borrowing Central Library First floor Baccah 547 PIR (Browse shelf(Opens below)) 173 Available 000043262
Total holds: 0

Includes bibliographical references and index.

1. Safety<br>2. Searching the literature<br>3. Reagents<br>4. Gases<br>5. Reactions on a small scale -- 1-25 mmol<br>6. Temperature control<br>7. Solvents<br>8. The research notebook<br>9. Conducting the reaction itself<br>10. Following the reaction<br>11. Working up reactions<br>12. Evaporation<br>13. Vacuum systems<br>14. Purification of products<br>15. Methods for structure elucidation<br>16. Cleaning up after the reaction<br>17. Specific examples<br>18. Strategies for reaction optimization<br>Appendices<br>1. Safety protocols<br>2. Synthetic solvent selection chart<br>3. Solvent miscibility<br>4. Freezing points of common organic solvents<br>5. Toxicities of common organic solvents<br>6. Recipes for TLC stains<br>7. NMR spectral data of common contaminants of organic and organometallic reaction products<br>8. Acidities of organic functional groups<br>9. Acidities of organic functional groups in DMSO<br>10. Stuck joints

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