Handbook of synthetic organic chemistry /

Pirrung, Michael.

Handbook of synthetic organic chemistry / Synthetic organic chemistry Michael C. Pirrung. - 2nd ed. - London : Academic Press, / Elsevier, c.2017. - xii, 272 p. : ill. (some col.) ; 24 cm.

Includes bibliographical references and index.

1. Safety
2. Searching the literature
3. Reagents
4. Gases
5. Reactions on a small scale -- 1-25 mmol
6. Temperature control
7. Solvents
8. The research notebook
9. Conducting the reaction itself
10. Following the reaction
11. Working up reactions
12. Evaporation
13. Vacuum systems
14. Purification of products
15. Methods for structure elucidation
16. Cleaning up after the reaction
17. Specific examples
18. Strategies for reaction optimization
Appendices
1. Safety protocols
2. Synthetic solvent selection chart
3. Solvent miscibility
4. Freezing points of common organic solvents
5. Toxicities of common organic solvents
6. Recipes for TLC stains
7. NMR spectral data of common contaminants of organic and organometallic reaction products
8. Acidities of organic functional groups
9. Acidities of organic functional groups in DMSO
10. Stuck joints

9780128095812


Organic compounds--Synthesis.





547 / PIR